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grits used which is prescribed in the definition and standard of identity therefor. [20 F.R. 9570, Dec. 20, 1955, as amended at 28 F.R. 6066, June 14, 1963] Subpart C-Rice and Related Products

§ 15.525 Enriched rice; identity; label statement of optional ingredients.

(a) The foods for which definitions and standards of identity are prescribed by this section are forms of milled rice (except rice coated with talc and glucose and known as coated rice), to which nutrients have been added so that each pound of the rice contains:

(1) Not less than 2.0 milligrams and not more than 4.0 milligrams of thiamine; not less than 1.2 milligrams and not more than 2.4 milligrams of riboflavin; not less than 16 milligrams and not more than 32 milligrams of niacin or niacinamide; and not less than 13 milligrams and not more than 26 milligrams of iron (Fe).

(2) Each pound may contain not less than 250 U. S. P. units and not more than 1,000 U. S. P. units of vitamin D.

(3) Each pound may contain not less than 500 milligrams and not more than 1,000 milligrams of calcium (Ca). Calcium carbonate derived from the use of this substance in milling rice, when present in quantities that furnish less than 500 milligrams of calcium (Ca) per pound, is considered a normal ingredient of the milled rice used and not an optional ingredient of the enriched rice unless such enriched rice is labeled to show it contains the optional ingredient calcium. Iron and calcium may be added only in forms that are harmless and assimilable. The vitamins referred to in subparagraphs (1) and (2) of this paragraph may be combined with harmless substances to render them insoluble in water, if the water-insoluble products are assimilable.

(4) In the case of enriched parboiled rice, butylated hydroxytoluene may be added as an optional ingredient in an amount not to exceed 0.0033 percent by weight of the finished food.

(b) The substances referred to in paragraph (a) (1), (2), and (3) of this section may be added in a harmless carrier. Such carrier is used only in the quantity necessary to effect an intimate and uniform mixture of such substances with the rice.

(c) Unless the label of the food bears the statement "To retain vitamins do not

rinse before or drain after cooking," immediately preceding or following the name of the food and in letters not less than one-fourth the point size of type used for printing the name of the food (but in no case less than 8-point type) and the label bears no cooking directions calling for washing or draining or unless the food is precooked and it is packaged in consumer packages which are conspicuously and prominently labeled with directions for preparation which, if followed, will avoid washing away or draining off enriching ingredients, the substances named in paragraph (a) (1), (2), and (3) of this section shall be present in such quantity or in such form that when the enriched rice is washed as prescribed in paragraph (e) of this section, the washed rice contains not less than 85 percent of the minimum quantities of the substances named in paragraph (a) (1) of this section, as required for enriched rice; and in case any optional ingredients named in paragraph (a) (2) and (3) of this section are used, the washed rice also contains not less than 85 percent of the minimum quantity specified for the substance or substances used.

(d) The name specified for each food for which a definition and standard of identity is prescribed by this section is the common name of the kind of milled rice to which the enriching substances are added, preceded by the word "enriched" as, for example, "Enriched rice" or "Enriched parboiled rice."

(e) The method referred to in paragraph (c) of this section is as follows: Mix the contents of one or more containers and transfer 1⁄2 pound thereof to a 4-liter flask containing 2 liters of distilled water at room temperature (but not below 20° C.). Stopper the flask and swirl it moderately for 2 minute so that the rice is in motion and in uniform suspension. Allow the rice to settle for 2 minute, then pour off 1,600 milliliters of the water, together with any floating and suspended matter, and discard. To the contents of the flask, add 1,600 milliliters of distilled water and 20 milliliters of 10 N hydrochloric acid. Agitate vigorously and wash down the sides of the flask with 150 milliliters of 0.1 N hydrochloric acid. In order to avoid excess foaming during the extraction, heat the mixture slowly to about 100° C., agitate gently if necessary, and maintain at this temperature until air is expelled. Again wash down the sides of the flask with 150 milliliters of 0.1 N

prominently and with such conspicuous-
ness (as compared with other words,
statements, designs, or devices in the
label) as to render it likely to be read
and understood by the ordinary individ-
ual under customary conditions of pur-
chase.

[22 F.R. 6887, Aug. 27, 1957, 22 FR. 6993,
Aug. 30, 1957, as amended at 23 FR. 1170,
Feb. 25, 1958, 25 F.R. 1686, Feb. 26, 1960, 25
FR. 3350, Apr. 19, 1960]

NOTE: The Order of the Commissioner of Food and Drugs appearing at 23 F.R. 1170, Feb. 25, 1958, amending paragraphs (a) (1) and (c) provides in part as follows: The regulations in § 15.525 are stayed insofar as they require each pound of the food to contain not less than 1.2 milligrams and not more than 2.4 milligrams of riboflavin. This stay shall continue until final action is taken disposing of the objections, after public hearing thereon.

PART 16-MACARONI AND NOODLE

Sec.
18.1

16.2

hydrochloric acid. Heat the mixture in
an autoclave at 120° C. to 123° C. for
30 minutes, remove and cool to room
temperature. Dilute the mixture with
distilled water so that the total volume
is 2,500 milliliters. Swirl the flask, and
while the solids are in uniform suspen-
sion pour off about 250 milliliters of the
mixture for later determination of iron
(and calcium, if this is to be deter-
mined). With filter paper that has been
shown not to adsorb thiamine, ribo-
flavin, or niacin, filter enough of the
remaining mixture for determination of
thiamine, riboflavin, and niacin. (In
the case of a mixture difficult to filter,
centrifuging or filtering through fritted
glass, or both, using a suitable analytical
filter-aid, may be substituted for, or may
precede, filtering through paper.) Di-
lute an aliquot of filtrate with 0.1 N hy-
drochloric acid, so that each milliliter
contains about 0.2 microgram of thia-
mine, and determine thiamine by the
method entitled "Rapid Fluorometric
Method-Official," beginning with sec-
tion 38.32 of the book "Official Methods
of Analysis of the Association of Official
Agricultural Chemists," 8th Edition,
1955. [Ed. note, 10th edition, 1965, p.
761, sec. 39.028.] With a suitable aliquot
determine riboflavin by the method en-
titled "Fluorometric Method-Official"
in the same book, beginning with the
third sentence of the second paragraph
in section 38.35(a), “Adjust, with vigor-
ous agitation *
[Ed. note, 10th
edition, 1965, p. 762, sec. 39.035.] De-
termine niacin in a 200-milliliter aliquot
of the filtrate by the method entitled
"Chemical Method-Official" in the same
book, beginning in the second sentence
of the first paragraph in section 38.47 16.8
(a), "adjust to pH 4.5 with
[Ed.
note, 10th edition, 1965, p. 763, sec.
39.038.1 Evaporate to dryness a 100-
milliliter aliquot of the nonfiltered ma-
terial withdrawn while agitating, and
determine iron using the method on page
208 of the same book entitled "Iron-Of-
ficial," [Ed. note, 10th edition, 1965, p.
192, secs. 13.011-13.013] and, if required
determine calcium as directed, on page
209 of the same book, entitled "Calcium-
Official." [Ed. note, 10th edition, 1965,
p. 193, sec. 13.014.]

33

(f) When the optional ingredient specified in paragraph (a) (4) of this section is added, the statement “Butylated hydroxytoluene added as a preservative" shall be placed on the label

16.3

16.4

16.5

16.6

16.7

16.9

PRODUCTS

Macaroni products; identity; label statement of optional ingredients. Milk macaroni products; identity; label statement of optional ingredients.

Whole wheat macaroni products; identity: label statement of optional ingredients.

Wheat and soy macaroni products; identity; label statement of optional Ingredients.

Vegetable macaroni products; identity; label statement of optional ingredients.

Noodle products; identity; label statement of optional ingredients. Wheat and soy noodle products; identity; label statement of optional ingredients.

Vegetable noodle products; identity; label statement of optional ingredients.

Enriched macaroni products; identity; label statement of optional ingredients.

16.10 Enriched noodle products; identity; label statement of optional ingredients.

16.11 Enriched vegetable macaroni products; identity; label statement of optional ingredients.

16.12 Enriched vegetable noodle products; identity; label statement of optional ingredients.

AUTHORITY: The provisions of this Part 16 issued under secs. 401, 701, 52 Stat. 1046, as amended, 1055, as amended; 21 U.S.C. 341, 371.

SOURCE: The provisions of this Part 16 appear at 20 F.R. 9575, Dec. 20, 1955, unless otherwise noted.

$16.1 Macaroni products; identity; la

bel statement of optional ingredients. (a) Macaroni products are the class of food each of which is prepared by drying formed units of dough made from semolina, durum flour, farina, flour, or any combination of two or more of these, with water and with or without one or more of the optional ingredients specified in subparagraphs (1) to (6), inclusive of this paragraph.

(1) Egg white, frozen egg white, dried egg white, or any two or all of these, in such quantity that the solids thereof is not less than 0.5 percent and not more than 2.0 percent of the weight of the finished food.

(2) Disodium phosphate, in a quantity not less than 0.5 percent and not more than 1.0 percent of the weight of the finished food.

(3) Onions, celery, garlic, bay leaf, or any two or more of these, in a quantity which seasons the food.

(4) Salt, in a quantity which seasons the food.

(5) Gum gluten, in such quantity that the protein content of the finished food is not more than 13 percent by weight. The finished macaroni product contains not less than 87 percent of total solids as determined by the method prescribed in "Official and Tentative Methods of Analysis of the Association of Official Agricultural Chemists," Fifth edition, 1940, page 235 [Ed. note, 10th edition, 1965, p. 209, sec. 13.115], under "Vacuum Oven Method-Official."

(6) Concentrated glyceryl monostearate (containing not less than 90 percent monoester), in a quantity not exceeding 2 percent by weight of the finished food.

(b) Macaroni is the macaroni product the units of which are tube-shaped and more than 0.11 inch but not more than 0.27 inch in diameter.

(c) Spaghetti is the macaroni product the units of which are tube-shaped or cord-shaped (not tubular) and more than 0.06 inch but not more than 0.11 inch in diameter.

(d) Vermicelli is the macaroni product the units of which are cord-shaped (not tubular) and not more than 0.06 inch in diameter.

(e) The name of each food for which a definition and standard of identity is prescribed by this section is "Macaroni Product"; or alternatively, the name is "Macaroni," "Spaghetti," or "Vermi

celli," as the case may be, when the units of the food are of the shapes and sizes specified in paragraph (b), (c), or (d), respectively, of this section.

(f) (1) When disodium phosphate is used the label shall bear the statement "Disodium phosphate added for quick cooking."

(2) When any ingredient specified in paragraph (a) (3) of this section is used the label shall bear the statement "Seasoned with------,” the blank being filled in with the common name of the ingredient; or in the case of bay leaves the statement "Spiced," "Spice added," or "Spiced with bay leaves."

(3) When the ingredient specified in paragraph (a) (6) of this section is used, the label shall bear the statement "Glyceryl monostearate added" or the statement "With added glyceryl monostearate."

(4) Wherever the name of the food appears on the label so conspicuously as to be easily seen under customary conditions of purchase, the words and statements prescribed in this section, showing the optional ingredients used, shall immediately and conspicuously precede or follow, or in part precede and in part follow, such name, without intervening written, printed, or graphic matter.

[20 F.R. 9575, Dec. 20, 1955, as amended at 29 F.R. 14074, Oct. 13, 1964, 29 F.R. 15643, Nov. 21, 1964]

§ 16.2

Milk macaroni products; identity; label statement of optional ingredients.

(a) Milk macaroni products are the class of food each of which conforms to the definition and standard of identity, and is subject to the requirements for label statement of optional ingredients, prescribed for macaroni products by § 16.1 (a) and (f) (2) and (3), except that:

(1) Milk is used as the sole moistening ingredient in preparing the dough; or in lieu of milk one or more of the milk ingredients specified in paragraph (f) of this section is used, with or without water, in such quantity that the weight of milk solids therein is not less than 3.8 percent of the weight of the finished milk macaroni product; and

(2) None of the optional ingredients permitted by § 16.1 (a) (1) and (2) is used. When the optional ingredient gum gluten (§ 16.1 (a) (5)) is added, the quantity is such that the protein derived therefrom, together with the protein de

rived from semolina, durum flour, farina, flour, or any combination of these used, does not exceed 13 percent of the weight of the finished food.

(b) Milk macaroni is the milk macaroni product the units of which conform to the specifications of shape and size prescribed for macaroni by § 16.1 (b).

(c) Milk spaghetti is the milk macaroni product the units of which conform to the specifications of shape and size prescribed for spaghetti by § 16.1 (c).

(d) Milk vermicelli is the milk macaroni product the units of which conform to the specifications of shape and size prescribed for vermicelli by § 16.1 (d).

(e) The name of each food for which a definition and standard of identity is prescribed by this section is "Milk Macaroni Product"; or alternatively, the name is "Milk Macaroni," "Milk Spaghetti," or "Milk Vermicelli," as the case may be, when the units of the food comply with the requirements of paragraph (b), (c), or (d), respectively, of this section.

(f) The milk ingredients referred to in paragraph (a) (1) of this section are concentrated milk, evaporated milk, dried milk, and a mixture of butter with skim milk, concentrated skim milk, evaporated skim milk, nonfat dry milk (dried skim milk), or any two or more of these, in such proportion that the weight of nonfat milk solids in such mixture is not more than 2.275 times the weight of milk fat therein.

[20 FR. 9576, Dec. 20, 1955, as amended at 21 FR. 6566, Aug. 31, 1956]

§ 16.3

Whole wheat macaroni products; identity; label statement of optional ingredients.

(a) Whole wheat macaroni products are the class of food each of which conforms to the definition and standard of identity, and is subject to the requirements for label statement of optional ingredients, prescribed for macaroni products by § 16.1 (a) and (f) (2) and (3), except that:

(1) Whole wheat flour or whole durum wheat flour or both are used as the sole wheat ingredient; and

(2) None of the optional ingredients permitted by § 16.1 (a) (1), (2), and (5) is used.

(b) Whole wheat macaroni is the whole wheat macaroni product the units

of which conform to the specifications of shape and size prescribed for macaroni by § 16.1 (b).

(c) Whole wheat spaghetti is the whole wheat macaroni product the units of which conform to the specifications of shape and size prescribed for spaghetti by § 16.1 (c).

(d) Whole wheat vermicelli is the whole wheat macaroni product the units of which conform to the specifications of shape and size prescribed for vermicelli by § 16.1 (d).

(e) The name of each food for which a definition and standard of identity is prescribed by this section is "Whole Wheat Macaroni Product"; or alternatively, the name is "Whole Wheat Macaroni," "Whole Wheat Spaghetti," or "Whole Wheat Vermicelli," as the case may be, when the units of the food comply with the requirements of paragraph (b), (c), or (d), respectively, of this section.

§ 16.4 Wheat and soy macaroni products; identity; label statement of optional ingredients.

(a) Wheat and soy macaroni products are the class of food each of which conforms to the definition and standard of identity, and is subject to the requirements for label statement of optional ingredients, prescribed for macaroni products by § 16.1 (a) and (f) (2) and (3), except that:

(1) Soy flour is added in a quantity not less than 12.5 percent of the combined weight of the wheat and soy ingredients used (the soy flour used is made from heat-processed, dehulled soybeans, with or without the removal of fat therefrom); and

(2) None of the optional ingredients permitted by § 16.1 (a) (1) and (2) is used. When the optional ingredient gum gluten (§ 16.1 (a) (5)) is added, the quantity is such that the protein derived therefrom, together with the protein derived from semolina, durum flour, farina, flour or any combination of these used, does not exceed 13 percent of the weight of the finished food.

(b) Wheat and soy macaroni is the wheat and soy macaroni product the units of which conform to the specifications of shape and size prescribed for macaroni by § 16.1 (b).

(c) Wheat and soy spaghetti is the wheat and soy macaroni product the units of which conform to the specifica

tions of shape and size prescribed for spaghetti by § 16.1 (c).

(d) Wheat and soy vermicelli is the wheat and soy macaroni product the units of which conform to the specifications of shape and size prescribed for vermicelli by § 16.1 (d).

(e) The name of each food for which a definition and standard of identity is prescribed by this section is "Wheat and Soy Macaroni Product," "Wheat and Soybean Macaroni Product," and Soy Macaroni Product," or

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and Soybean Macaroni Product," the blank in each instance being filled in with the name whereby the wheat ingredient used is designated in § 16.1 (a); or alternatively, the name is "Wheat and Soy Macaroni,' ," "Wheat and Soybean Macaroni," and Soy Macaroni," or" and Soybean Macaroni" when the units of the food comply with the requirements of paragraph (b) of this section; or "Wheat and Soy Spaghetti," "Wheat and Soybean Spaghetti," and Soy Spaghetti," or and Soybean Spaghetti" when such units comply with the requirements of paragraph (c) of this section; or "Wheat and Soy Vermicelli," "Wheat and Soybean Vermicelli," and Soy Vermicelli," or ". and Soybean Vermicelli" when such units comply with the requirements of paragraph (d) of this section, the blank in each instance being filled in with the name whereby the wheat ingredient used is designated in § 16.1 (a).

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§ 16.5 Vegetable macaroni products; identity; label statement of optional ingredients.

(a) Vegetable macaroni products are the class of food each of which conforms to the definition and standard of identity, and is subject to the requirements for label statement of optional ingredients, prescribed for macaroni products by § 16.1 (a) and (f) (2) and (3), except that:

(1) Tomato (of any red variety), artichoke, beet, carrot, parsley, or spinach is added in such quantity that the solids thereof is not less than 3 percent by weight of the finished vegetable macaroni product (the vegetable used may be fresh, canned, dried, or in the form of puree or paste); and

(2) None of the optional ingredients permitted by § 16.1 (a) (1) and (2) is used. When the optional ingredient gum

gluten (§16.1 (a) (5)) is added, the quantity is such that the protein derived therefrom, together with the protein derived from the semolina, durum flour, farina, flour or any combination of these used, does not exceed 13 percent of the weight of the finished food.

(b) Vegetable macaroni is the vegetable macaroni product the units of which conform to the specifications of shape and size prescribed for macaroni by § 16.1 (b).

(c) Vegetable spaghetti is the vegetable macaroni product the units of which conform to the specifications of shape and size prescribed for spaghetti by § 16.1 (c).

(d) Vegetable vermicelli is the vegetable macaroni product, the units of which conform to the specifications of shape and size prescribed for vermicelli by § 16.1 (d).

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(e) The name of each food for which a definition and standard of identity is prescribed by this section is ". Macaroni Product," the blank being filled in with the name whereby the vegetable used is designated in paragraph (a) of this section; or alternatively, the name is Macaroni," Spaghetti," Vermicelli," as the case may be, when the units of the food comply with the requirements of paragraph (b), (c), or (d), respectively, the blank in each instance being filled in with the name whereby the vegetable used is designated in paragraph (a) of this section. § 16.6 Noodle products; identity; label statement of optional ingredients.

(a) Noodle products are the class of food each of which is prepared by drying formed units of dough made from semolina, durum flour, farina, flour, or any combination of two or more of these, with liquid eggs, frozen eggs, dried eggs, egg yolks, frozen yolks, dried yolks, or any combination of two or more of these, with or without water and with or without one or more of the optional ingredients specified in subparagraphs (1) to (4), inclusive:

(1) Onions, celery, garlic, bay leaf, or any two or more of these, in a quantity which seasons the food.

(2) Salt, in a quantity which seasons the food.

(3) Gum gluten, in such quantity that the protein derived therefrom, together with the protein derived from semolina, durum flour, farina, flour or any combi

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